HRID1278187

反应详情

EQUATION

反应方程式

HRID 1278187 的结构方程式

PROCEDURE

实验过程

To a solution of 2-chloro-6-fluorobenzamidocarboxylic acid, 4-nitrophenyl ester, in an inert organic solvent is added 5-bromo-2-aminopyridine. The reaction mixture is stirred at an elevated temperature for a period of time, and is then evaporated to dryness under vacuum. The product named in the heading above, identical to the product of Example 2, is isolated and purified by recrystallization.

WORKUP

后处理

  1. customis then evaporated to dryness under vacuum
  2. customis isolated
  3. custompurified by recrystallization