HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one → HCID 11392298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one | HCID 567033 | — |
| Reactant | Ethyl 3-amino-5-ethyl-1H-pyrazole-4-carboxylate | HCID 15186424 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 11392298 | HCID 11392298 | — |
Reaction Steps
As for Example 2, 1.83 g. of 3-amino-4-carboethoxy-5-ethylpyrazole is heated at reflux temperature for 16 hours with 1.76 g. of 3-dimethylamino-1-(3-pyridyl)-2-propen-1-one in 25 ml. of glacial acetic acid to give 1.20 g. of the product of the example as colorless crystals, m.p. 119°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04281000 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-09574af49c5f4b9d887acc7b291c5df2 |
| Source note | uspto-grants-1981_07 |