HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Dimethylamino-1-thien-3-ylpropen-1-one → 3-Bromo-7-(3-thienyl)pyrazolo[1,5-a]pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Dimethylamino-1-thien-3-ylpropen-1-one | HCID 596466 | — |
| Reactant | HCID 178509245 | HCID 178509245 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 3-Bromo-7-(3-thienyl)pyrazolo[1,5-a]pyrimidine | HCID 21163084 | — |
Reaction Steps
A mixture of 0.01 mole of 3-dimethylamino-1-(3-thienyl)-2-propen-1-one and 0.01 mole of 3-amino-4-bromopyrazole in glacial acetic acid is heated at reflux temperature for 8 hours. The solvent is removed in vacuo to give the product of the example.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04281000 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-beb2d02e5c714b68af21a308ee9700bf |
| Source note | uspto-grants-1981_07 |