Carbon Disulfide → HCID 524151, compound

Participants

Reaction Steps

9.7 Grams of diethylamine was added to 50 ml of tetrahydrofuran, and while maintaining the mixture at a temperature of 0°-5° C. and under agitation, 5.0 gr of carbon disulfide was added dropwise to the mixture over the period of 30 minutes. Thereafter, the temperature of the mixture was allowed to rise up to a room temperature, followed by dropwise addition of 4.6 gr of allyl chloride over the period of 30 minutes. The reaction mixture was poured into water and the separated organic substance was extracted twice with 30 ml of toluene, washed with diluted hydrochloric acid and further washed with water. After removal of toluene by distillation, there was obtained 8.3 gr of the desired product.

Provenance & Evidence