HRID1278301

反应详情

EQUATION

反应方程式

HRID 1278301 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 3.62 g. of 4-(allylamino)phenylacetic acid and 25 ml. of ethanol water (9:1) containing 0.400 g. of sodium hydroxide is stirred for 4 hours. The mixture is filtered and the residue washed with 10 ml. of ethanol-water (9:1) and dried in vacuo for 24 hours to yield sodium 4-(allylamino)phenylacetate as a white solid.

WORKUP

后处理

  1. additionA mixture of 3.62 g
  2. filtrationThe mixture is filtered
  3. washthe residue washed with 10 ml
  4. dry with materialof ethanol-water (9:1) and dried in vacuo for 24 hours