HCID 12275522, compound → HCID 21163975, compound

HRID 1278361Notes

Reaction equation

HRID 1278361 reaction equation
[CH3:1][C:2]([CH3:6])([S:4]Cl)[CH3:3].[NH:7]1[C:11](=[O:12])[C:10](=[O:13])[NH:9][C:8]1=[O:14].[Na]>>[C:2]([S:4][N:7]1[C:11](=[O:12])[C:10](=[O:13])[NH:9][C:8]1=[O:14])([CH3:6])([CH3:3])[CH3:1]

Participants

3

Reactant 2

HCID 12275522HCID 12275522, compoundHCID 70578064HCID 70578064, compound

Product 1

HCID 21163975HCID 21163975, compound

Procedure

1-(t-Butylthio)imidazolidinetrione is prepared by adding a solution of 1,1-dimethylethane sulfenyl chloride (0.1 mole) to a stirred slurry of sodium imidazolidinetrione (0.1 mole). 1-(t-Butylthio)imidazolidinetrione, m.p. 150.5°-152° C. recrystallized from toluene, is recovered.

Workup

  1. custom1-(t-Butylthio)imidazolidinetrione, m.p. 150.5°-152° C. recrystallized from toluene
  2. customis recovered

Sources & evidence

ORD record
ord-026ff3210eca47c8bcb4149399a1363b
Source dataset
uspto-grants-1981_07
Patent number
US04281139

Reaction notes

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