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HRID1278367

反应详情

EQUATION

反应方程式

HRID 1278367 的结构方程式

REACTANTS

反应物

2
结构：C[O+](C)C.[Cl][Sb-]([Cl])([Cl])([Cl])([Cl])[Cl]
HCID150258

Trimethyloxonium hexachloroantimonate

C3H9Cl6OSb

结构：Clc1nsc(Cl)c1Cl
HCID12333154

未命名化合物

PRODUCTS

生成物

1
结构：C[n+]1sc(Cl)c(Cl)c1Cl.[Cl][Sb-]([Cl])([Cl])([Cl])([Cl])[Cl]
HCID16695738

未命名化合物

收率 73%

PROCEDURE

实验过程

Trichloroisothiazole (10 ml) and trimethyloxonium hexachloroantimonate (7.9 g, 0.02 mol) were heated at 90° for 30 min. After cooling either (150 ml) was added and the solid collected to yield 7.8 g (73%) of product, mp >240. Spectral data (NMR & IR) were consistent with the assigned structure.

WORKUP

后处理

  1. temperatureAfter cooling either (150 ml)
  2. additionwas added
  3. customthe solid collected