HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → HCID 54402546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | Ethane, 1,2-dichloro-1-methoxy- | HCID 162049 | — |
| Product | HCID 54402546 | HCID 54402546 | 57.8% |
Reaction Steps
0.9 mole of methyl 1,2-dichloroethyl ether was added dropwise to 1 mole of triethyl phosphite at 120° C., under a N2 atmosphere. After a reaction time of 8 hours, the mixture was fractionated. 120 g of 1-methoxy-2-chloroethane-phosphonic acid diethyl ester were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04257987 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-a922a4b4c5f14e849b0a4e4023bb40db |
| Source note | uspto-grants-1981_03 |