HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 85060166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 85065263 | HCID 85065263 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 85060166 | HCID 85060166 | — |
Reaction Steps
In a manner similar to that of Example 2, by reaction of 600 mg of ethyl 3-methyl-5-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-ylselenyl)-pent-2-en-4-ynoate with 600 mg of LiOH in 15 ml of THF, 410 mg (73%) of a yellow powder are obtained. m.p.: 175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06444709B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-26f464493973467dbeb5da967094a271 |
| Source note | uspto-grants-2002_09 |