HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromoisoquinoline → 7-Bromoisoquinoline N-oxide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromoisoquinoline | HCID 736487 | — |
| Reactant | 7-Bromoisoquinoline | HCID 12257441 | — |
| Reactant | 6-Bromoisoquinoline N-oxide hydrochloride | HCID 22665630 | — |
| Reactant | 5-bromoisoquinoline N-oxide hydrochloride | HCID 22665707 | — |
| Product | 7-Bromoisoquinoline N-oxide hydrochloride | HCID 22665926 | — |
Reaction Steps
Compound 37a was prepared from 7-bromoisoquinoline (Tyson, F. L., J. Am. Chem. Soc. 61, 183 (1939), this procedure gave a mixture of 7-bromoisoquinoline and 5-bromoisoquinoline) using the procedure described for 1a. The title compound was contaminated with the 5-bromo-isoquinoline N-oxide hydrochloride. M.p. 107.0-112.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06444672B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-a839a4bcdbed4313aa6e1720c83202e1 |
| Source note | uspto-grants-2002_09 |