HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → 7-Methoxy-2,3-dihydro-5H-benzo[f][1,4]oxazepine-4-sulfonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 7-methoxy-3,4-dihydro-1H-isoquinoline-2-sulfonyl chloride | HCID 22665676 | — |
| Reactant | 7-Methoxy-2,3,4,5-tetrahydro-1,4-benzoxazepine | HCID 22665820 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 7-Methoxy-2,3-dihydro-5H-benzo[f][1,4]oxazepine-4-sulfonyl chloride | HCID 22665621 | — |
Reaction Steps
This compound was prepared from 1.4 g of 7-methoxy-2,3,4,5-tetrahydro-benzo[f][1,4]-oxazepine, 0.91 mL of sulfuryl chloride and 4.7 mL of triethylamine using the procedure described for 63f. Yield: 0.23 g (oil), EI-MS: 277 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06444672B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-e2e9ca3ce81b412ca706580edc49e135 |
| Source note | uspto-grants-2002_09 |