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HRID1279121

反应详情

EQUATION

反应方程式

HRID 1279121 的结构方程式

REACTANTS

反应物

2
结构：Cl.O=C(OCc1ccccc1)[C@@H]1CCCN1
HCID2733413

Benzyl L-prolinate hydrochloride

C12H16ClNO2

结构：COc1ccc(C[C@@H](NC(=O)OC(C)(C)C)C(=O)O)cc1
HCID7017908

BOC-O-METHYL-D-TYROSINE

C15H21NO5

PRODUCTS

生成物

1
结构：COc1ccc(C[C@@H](NC(=O)OC(C)(C)C)C(=O)N2CCC[C@H]2C(=O)OCc2ccccc2)cc1
HCID69780134

未命名化合物

收率 52.5%

PROCEDURE

实验过程

Reaction of 3.5 g of N-tert.-Butoxycarbonyl-2-(R)-amino-3-(4-methoxyphenyl)-propionic acid and 2.9 g of (L)-proline benzyl ester hydrochloride according to the procedure described for example 91b gave 3.0 g (52%) of the title compound as a yellow oil. (+)-APCI-MS: 505 (MNa+).