HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phytol → Dihydrophytol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phytol | HCID 5280435 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Dihydrophytol | HCID 102459 | — |
Reaction Steps
Phytol (5.0 g, 16.7 mmol) was stirred in ethanol (50 mL) in the presence of Raney nickel (1.0 g, 50% slurry in water) overnight under H2 atmosphere. The catalyst was filtered off and the solvent evaporated to give a clear oil. Yield: 4.9 g (97%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06447656B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-bb96f606cf8d439a9ce4a1a44d001ba2 |
| Source note | uspto-grants-2002_09 |