HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 18343913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 3662321 | HCID 3662321 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18343913 | HCID 18343913 | 82.8% |
Reaction Steps
A mixture of 10.0 g (0.044 mol) of 1-oxyl-2,2,6,6-tetramethyl-4-glycidyloxypiperidine and 10 mL of 40% (ca. 0.091 mol) of dimethylamine (w/w) is dissolved in 100 mL of water and then stirred for 16 hours at ambient temperature. Water is then removed by vacuum distillation to leave 10 g of the title compound as a red oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06447644B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-6d9979b793024bb3b19f022e2d9f851c |
| Source note | uspto-grants-2002_09 |