HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 17896515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 1,4-Dihydroxy-2,2,6,6-tetramethylpiperidine | HCID 5395 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 17896515 | HCID 17896515 | 59.1% |
Reaction Steps
5.0 g (0.029 mol) 1-hydroxy-2,2,6,6-tetramethyl-4-hydroxypiperidine and 2.0 g (0.033 mol) acetic acid are recrystallized from 50 mL of isopropanol, yielding 4.0 g of the desired hydroxylamine salt as a white crystalline solid, mp 140-143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06447644B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-b558339ada8346ec860997b06b035df5 |
| Source note | uspto-grants-2002_09 |