HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-3-Hydroxypyridine → HCID 178476690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-3-Hydroxypyridine | HCID 28114 | — |
| Reactant | HCID 178475853 | HCID 178475853 | — |
| Product | HCID 178476690 | HCID 178476690 | — |
Reaction Steps
The method of preparation of 2-imino-3-methylpiperidine acetate, EXAMPLE 6, was used to convert 2-amino-3-hydroxypyridine to the title compound which was obtained as a white solid. The analysis of the product was found to be consistent with the proposed structure. m.p. 128-130° C. MH+=115 ; 1H NMR (D2O): δ4.34-4.28 (m, 1H); 3.20-3.10 (m, 2H); 2.05-1.50 (m, 4H); 1.71 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448286B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-ad6ac48be26c497faf97afbd988053e6 |
| Source note | uspto-grants-2002_09 |