Ammonium Chloride → HCID 178440909, compound

HRID 1279514Notes

Reaction equation

HRID 1279514 reaction equation
[CH3:1][C:2]([CH:5]1[C:11](OC)=[N:10][CH2:9][CH2:8][CH2:7][CH2:6]1)([CH3:4])[CH3:3].[Cl-:14].[NH4+:15]>CO>[ClH:14].[CH3:1][C:2]([CH:5]1[CH2:6][CH2:7][CH2:8][CH2:9][NH:10][C:11]1=[NH:15])([CH3:4])[CH3:3]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 18428484HCID 18428484, compound

Product 1

HCID 178440909HCID 178440909, compoundYield 63.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 99 (551 mg, 2.7 mmol) in 10 mL of MeOH was reacted with ammonium chloride (145 mg, 2.7 mmol) by the method of EXAMPLE 27 to yield 350 mg of the crude title material.

Sources & evidence

ORD record
ord-cd5912b1a8f94086a10ce16669b7603d
Source dataset
uspto-grants-2002_09
Patent number
US06448286B1

Reaction notes

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