Ammonium Chloride → HCID 178442371, compound

HRID 1279536Notes

Reaction equation

HRID 1279536 reaction equation
[CH2:1]([CH:3]([CH2:14][CH3:15])[CH2:4][CH:5]1[CH2:11][CH2:10][CH2:9][CH2:8][C:7](OC)=[N:6]1)[CH3:2].[Cl-:16].[NH4+:17]>CO>[ClH:16].[CH2:1]([CH:3]([CH2:14][CH3:15])[CH2:4][CH:5]1[NH:6][C:7](=[NH:17])[CH2:8][CH2:9][CH2:10][CH2:11]1)[CH3:2]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 10750993HCID 10750993, compound

Product 1

HCID 178442371HCID 178442371, compoundYield 57.8%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 196 (470 mg, 2.2 mmol) in 18 mL of MeOH was reacted with ammonium chloride (98 mg, 1.8 mmol) by the method of EXAMPLE 27 to yield 242 mg of the title material.

Sources & evidence

ORD record
ord-fc7e52738d714d6fb01fd4a16d18f203
Source dataset
uspto-grants-2002_09
Patent number
US06448286B1

Reaction notes

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