Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18428508, compound

HRID 1279551Notes

Reaction equation

HRID 1279551 reaction equation
[O:1]=[C:2]1[NH:8][CH:7]([CH2:9][CH2:10][CH2:11][CH:12]([NH:18][C:19]([O:21][CH2:22][C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)=[O:20])[C:13]([O:15][CH2:16][CH3:17])=[O:14])[CH2:6][CH2:5][CH2:4][CH2:3]1.F[B-](F)(F)F.[CH3:34][O+](C)C>C(Cl)Cl>[CH3:34][O:1][C:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH:7]([CH2:9][CH2:10][CH2:11][CH:12]([NH:18][C:19]([O:21][CH2:22][C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)=[O:20])[C:13]([O:15][CH2:16][CH3:17])=[O:14])[N:8]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 18428458HCID 18428458, compound

Product 1

HCID 18428508HCID 18428508, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of EXAMPLE 247 is treated with trimethyloxonium tetraflouroborate in CH2Cl2 by the method of EXAMPLE 26 to yield title material.

Workup

  1. customto yield title material

Sources & evidence

ORD record
ord-fdc46a645bb24517890488f4d4454887
Source dataset
uspto-grants-2002_09
Patent number
US06448286B1

Reaction notes

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