Ammonium Chloride → HCID 178428696, compound

HRID 1279558Notes

Reaction equation

HRID 1279558 reaction equation
CO[C:3]1[CH2:4][CH:5]([CH3:26])[CH:6]([CH2:8][CH2:9][CH2:10][CH:11]([NH:18]C(=O)OC(C)(C)C)[CH:12]2[CH2:16][O:15][C:14](=[O:17])[O:13]2)[N:7]=1.[Cl-:27].[NH4+:28].Cl.CCOC(C)=O>CO>[ClH:27].[ClH:27].[NH2:18][CH:11]([CH:12]1[CH2:16][O:15][C:14](=[O:17])[O:13]1)[CH2:10][CH2:9][CH2:8][CH:6]1[CH:5]([CH3:26])[CH2:4][C:3](=[NH:28])[NH:7]1

Participants

5

Reactant 3

HCID 25517Ammonium ChlorideHCID 18428551HCID 18428551, compoundHCID 21866389Hydrogen chloride-ethyl acetate

Product 1

HCID 178428696HCID 178428696, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 262 in MeOH is reacted with ammonium chloride by the method of EXAMPLE 27, then teated with 3M HCl/EtOAc to generate the title material.

Sources & evidence

ORD record
ord-aa03834ac0d146be937b05ce52255c76
Source dataset
uspto-grants-2002_09
Patent number
US06448286B1

Reaction notes

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