HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 1-Cyclohexyl-1-phenyl-hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | N-Cyclohexylaniline | HCID 74567 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | N-Cyclohexyl-N-phenylnitrous amide | HCID 23471014 | — |
| Product | 1-Cyclohexyl-1-phenyl-hydrazine | HCID 12866328 | — |
Reaction Steps
N-Cyclohexyl-N-nitrosoaniline, prepared from N-cyclohexylaniline by the method described in Example 1 was subsequently reduced to the hydrazine by the lithium aluminum hydride method described in Example 4. 1-Cyclohexyl-1-phenyl hydrazine distilled at 120°-150° C./0.2 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04258059 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-1359a50870784657a2321d5ed8fa712e |
| Source note | uspto-grants-1981_03 |