Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | 2-Hydroxyethyl acrylate | HCID 13165 | — |
| Reactant | Isooctyl acrylate | HCID 165746 | — |
| Reactant | Isobomyl acrylate | HCID 92004758 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Ioa iba hea | HCID 131723480 | — |
Reaction Steps
In a glass polymerization bottle were charged 80 g isooctyl acrylate (IOA), 18 g isobornyl acrylate (IBA), 2 g 2-hydroxyethyl acrylate (HEA), 100 g ethyl acetate, 0.5 g benzoyl peroxide and 0.04 g carbon tetrabromide. The bottle was purged with nitrogen, sealed and tumbled in a water bath maintained at 60° C. for 12 hours to produce an IOA/IBA/HEA terpolymer. The polymer was isolated by precipitation in methanol and dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06448337B1 |
|---|
| Source dataset | uspto-grants-2002_09 |
|---|
| ORD ID | ord-1525d0c9b5794d729a2e340409a600c2 |
|---|
| Source note | uspto-grants-2002_09 |
|---|
