HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → 5,10,15,20-tetra(2-hydroxyphenyl)porphyrin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | Pyrrole | HCID 8027 | — |
| Solvent | Propionic Acid | HCID 1032 | — |
| Product | 5,10,15,20-tetra(2-hydroxyphenyl)porphyrin | HCID 135474844 | — |
Reaction Steps
Pyrrole (1.0 equivalents) and salicylaldehyde (1.2 equivalents) are dissolved in propionic acid (1 liter/20 ml pyrrole) and the solution is refluxed for 30 minutes. The reaction mixture is allowed to cool to room temperature and stand for one day. The mixture is filtered and the product is recrystallized to yield 5,10,15,20-tetrakis(2′-hydroxyphenyl) porphyrin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448414B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-dbbe931ef3a6426fb298be071b777309 |
| Source note | uspto-grants-2002_09 |