2-(4-Chlorophenyl)ethane-1-sulfonyl chloride → HCID 23471001, compound

HRID 127977Notes

Reaction equation

HRID 127977 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][S:10](Cl)(=[O:12])=[O:11])=[CH:4][CH:3]=1.[NH2:14][CH2:15][CH2:16][C:17]1[CH:31]=[CH:30][C:20]([O:21][C:22]([CH3:29])([CH3:28])[C:23]([O:25][CH2:26][CH3:27])=[O:24])=[CH:19][CH:18]=1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][S:10]([NH:14][CH2:15][CH2:16][C:17]2[CH:18]=[CH:19][C:20]([O:21][C:22]([CH3:28])([CH3:29])[C:23]([O:25][CH2:26][CH3:27])=[O:24])=[CH:30][CH:31]=2)(=[O:12])=[O:11])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 27577802-(4-Chlorophenyl)ethane-1-sulfonyl chlorideHCID 19356632Ethyl 2-[4-(2-aminoethyl)-phenoxy]-2-methylpropionate

Product 1

HCID 23471001HCID 23471001, compoundYield 77%

Procedure

from 2-(4-chlorophenyl)-ethanesulphonyl chloride and ethyl 2-[4-(2-aminoethyl)-phenoxy]-2-methylpropionate; colorless oil; yield 77% of theory, and from this, by hydrolysis:

Workup

  1. customyield 77% of theory, and from this, by hydrolysis

Sources & evidence

ORD record
ord-0c73c13dc8d343ad8d4db3f85d76e020
Source dataset
uspto-grants-1981_03
Patent number
US04258058

Reaction notes

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