HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Benzenediazonium, 4-methoxy-, chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Solvent | Water | HCID 962 | — |
| Product | Benzenediazonium, 4-methoxy-, chloride | HCID 11829892 | 77% |
Reaction Steps
A solution of 4-methoxy-phenyl-diazonium chloride was prepared by adding dropwise at 0° C. a solution of 1.8 g of sodium nitrite dissolved in 2.5 ml of water to a solution of 3.075 g of p-anisidine dissolved in 25 ml of water and 8.1 ml of concentrated hydrochloric acid. The reaction mixture was allowed to stand for 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04258120 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-3bf2fabb883b43b583957c7643dfea67 |
| Source note | uspto-grants-1981_03 |