HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetoxyacetyl chloride → HCID 18429273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetoxyacetyl chloride | HCID 26297 | — |
| Reactant | HCID 18429214 | HCID 18429214 | — |
| Product | HCID 18429273 | HCID 18429273 | — |
Reaction Steps
1-(1,2-Dihydroxyethyl)-3,5-diamino-2,4,6-triiodobenzene is acylated with acetoxyacetyl chloride using for example such a procedure as described in Example 4d. The crude product is then hydrolyzed analogous to Example 4e to give the final product. Purification of the crude product is carried out using preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448442B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-9f4d8d8d8584489c9b4074e650328a58 |
| Source note | uspto-grants-2002_09 |