HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → 5-Amino-3-acetoxymethyl-N,N-bis(2-hydroxyethyl)-2,4,6-triiodobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 5-Amino-3-acetoxymethyl-2,4,6-triiodobenzoyl chloride | HCID 18429338 | — |
| Product | 5-Amino-3-acetoxymethyl-N,N-bis(2-hydroxyethyl)-2,4,6-triiodobenzamide | HCID 18429242 | — |
Reaction Steps
5-Amino-3-acetoxymethyl-2,4,6-triiodobenzoyl chloride was reacted with diethanolamine according to the general procedure in Example 24 g. Yield of isolated crude product was 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448442B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-94bcc3ee12384058802bfd0c5e68efaf |
| Source note | uspto-grants-2002_09 |