HRID1280182

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID14798

Sodium Hydroxide

HNaO

反应SMILES：CC(=O)OCc1c(I)c(NC(=O)C(OC(C)=O)C(COC(C)=O)OC(C)=O)c(I)c(C(=O)NCC(COC(C)=O)OC(C)=O)c1I

HCID18429174

未命名化合物

PRODUCTS

产物

反应SMILES：O=C(NCC(O)CO)c1c(I)c(CO)c(I)c(NC(=O)C(O)C(O)CO)c1I

HCID9918386

未命名化合物

收率 68%

PROCEDURE

实验过程

5-[N′-(2,3,4-Triacetoxybutanoyl)amino]-3-acetoxymethyl-N-(2,3-diacetoxypropyl)-2,4,6-triiodobenzamide (13.8 g, 14.0 mmol) was hydrolysed using sodium hydroxide (4.0 g, 0.10 mol) according to the procedure given in Example 79c. The product was isolated in 68% yield after purification.

WORKUP

后处理

customThe product was isolated in 68% yield
customafter purification