2-Bromo-4-(bromomethyl)benzenemethanol → 2-Bromo-4-(bromomethyl)benzaldehyde

Beteiligte Stoffe

Reaktionsschritte

The compound of Step 2 (8 g, 29 mmol, 1 eq) was dissolved in 10% EtOH/EtOAc (300 ml) and 5 eq of MnO2 (12.4 g, 142 mmol) was added every hour for 6 hours. The mixture was filtered through Celite and the solvent was removed under vacuum to give 6.5 g (80%) of the title compound.

Herkunft & Nachweise