Methylhydrazine → HCID 18425032, compound

HRID 1280323Notes

Reaction equation

HRID 1280323 reaction equation
[Cl:1][C:2]1[C:7]([Cl:8])=[C:6]([O:9][CH3:10])[CH:5]=[CH:4][C:3]=1[CH2:11][C:12](=O)[CH2:13][C:14]([O:16]C)=O.[CH3:19][NH:20][NH2:21]>>[Cl:1][C:2]1[C:7]([Cl:8])=[C:6]([O:9][CH3:10])[CH:5]=[CH:4][C:3]=1[CH2:11][C:12]1[NH:21][N:20]([CH3:19])[C:14](=[O:16])[CH:13]=1

Participants

3

Reactant 2

HCID 6061MethylhydrazineHCID 18425030HCID 18425030, compound

Product 1

HCID 18425032HCID 18425032, compound

Procedure

46.2 g (0.16 mol) of methyl 4-(2,3-dichloro-4-methoxyphenyl)-3-oxobutyrate and 8.1 g (0.18 mol) of methylhydrazine were reacted by the method of Example 1. Yield: 30.8 g;

Sources & evidence

ORD record
ord-033b5f8959e441309bf8bb26d48bbe43
Source dataset
uspto-grants-2002_09
Patent number
US06451734B1

Reaction notes

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