HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → N-(4-Nitrophenyl)hydrazinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | phenyl 4-nitrophenylcarbamate | HCID 11322856 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | N-(4-Nitrophenyl)hydrazinecarboxamide | HCID 12467017 | — |
Reaction Steps
Hydrazine (1.18 mol) was added dropwise over a 1 hour period to a solution of intermediate (1) in 1,4-dioxane (1000 ml) and the mixture was stirred and refluxed overnight. The mixture was cooled and filtered off, yielding N-(4-nitro-phenyl)hydrazinecarboxamide (intermediate 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451802B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-4947ae4ea09a4d879cbc317be6233219 |
| Source note | uspto-grants-2002_09 |