HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine, sulfate (1:1) → Sulfuric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine, sulfate (1:1) | HCID 159255 | — |
| Reactant | 3,3-Dimethyl-12-ethyl-1-aza-1,5,9-cyclododecatriene | HCID 53743254 | — |
| Product | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 20405361 | HCID 20405361 | — |
| Product | HCID 73665703 | HCID 73665703 | — |
Reaction Steps
Reaction of 3,3-dimethyl-12-ethyl-1-aza-1,5,9-cyclododecatriene with hydroxylamine sulfate, in the presence of sulfuric acid, to 2,2-dimethyl-11-ethyl-11-aminoundeca-4,8-dienal-oxime, and hydrogenation of this to give 1-ethyl-10,10-dimethyl-1,11-diaminoundecane; b.p. 93° C./7 Pa; nD20 =1.4622.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04258176 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-938d3f7f5a334364846156cd7a5a94f4 |
| Source note | uspto-grants-1981_03 |