HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzenethiol → (RS)-3-(3-Methoxy-phenylsulfanyl)-1-(toluene-4-sulfonyl)-pyrrolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzenethiol | HCID 84989 | — |
| Reactant | 1-Tosyl-3-pyrrolidinol Tosylate | HCID 15020355 | — |
| Product | (RS)-3-(3-Methoxy-phenylsulfanyl)-1-(toluene-4-sulfonyl)-pyrrolidine | HCID 18425858 | — |
Reaction Steps
The title compound, MS: m/e=363.1 (M+) was prepared from (RS)-toluene-4-sulfonic acid 1-(toluene-4-sulfonyl)-pyrrolidin-3-yl ester and 3-methoxythiophenol and by using DMF as solvent instead of acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451819B2 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-d7cef4d011a84ccc9a08d6a00e4457f5 |
| Source note | uspto-grants-2002_09 |