HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53640826, compound → HCID 9846245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53640826 | HCID 53640826 | — |
| Solvent | MeOH tetrahydrofuran | HCID 21899815 | — |
| Product | HCID 9846245 | HCID 9846245 | 53.6% |
Reaction Steps
[[2-Ethyl-1-(2-phenyl-phenylmethyl)-3-ureido-1H-indol-4-yl]oxy]acetic acid tert-butyl ester (0.206 g) was treated with 5 mL of a 7:1 mixture of methanol/tetrahydrofuran at room temperature overnight. After concentrating to dryness and adding 1 mL of 1N HCl, stirring was continued at room temperature for an hour. The resulting solid was filtered off and vacuum dried to provide 0.098 g of [[2-ethyl-1-(2-phenyl-phenylmethyl)-3-ureido-1H-indol-4-yl]oxy]acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451839B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-a8723c44c9274c8d9dc05debcc58bdfc |
| Source note | uspto-grants-2002_09 |