Tin tetrachloride → HCID 21193478, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure in Example 5, step 2 using 3-cyclopentyl-p-anisic acid (10.0 g, 45.5 mmol, RN-59216-82-9), oxalyl chloride (4.4 mL, 50.6 mmol), N,N-dimethylformamide (2 drops), tin (IV) chloride (15.8 mL, 49.6 mmol) and 2-benzyl-4,5-dimethyl-furan (10.1 g, 54.3 mmol) in CH2Cl2 to give 18.8 g (crude) of the title compound. 1H NMR (DMSO-d6) consistent.

Provenance & Evidence