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(3,4-Dimethoxyphenyl)hydrazine → 3-(Dimethylamino)-6,7-dimethoxy-1,2,3,4-tetrahydrocarbazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (3,4-Dimethoxyphenyl)hydrazine | HCID 88491 | — |
| 反応物 | 4-(Benzoyloxy)cyclohexanone | HCID 242677 | — |
| 反応物 | 3-Benzoyloxy-6,7-dimethoxy-1,2,3,4-tetrahydrocarbazole | HCID 12891777 | — |
| 生成物 | 3-(Dimethylamino)-6,7-dimethoxy-1,2,3,4-tetrahydrocarbazole | HCID 12891776 | — |
反応手順
The 3-benzoyloxy-6,7-dimethoxy-1,2,3,4-tetrahydrocarbazole, m.p. 123°-125° C., was prepared from 102 g. of 3,4-dimethoxyphenylhydrazine and 109 g. of 4-benzoyloxycyclohexanone by following a procedure similar to that described in Example 3.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04257952 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-3016c80a73044ea29248ddf7cecc3131 |
| 出典メモ | uspto-grants-1981_03 |