HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12361802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1H-Carbazol-3-amine, 2,3,4,9-tetrahydro-N,N,6,8-tetramethyl-, hydrochloride (1:1) | HCID 12361803 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12361802 | HCID 12361802 | — |
Reaction Steps
Following the procedure given in Example 3 and using 9 g. of 4-dimethylaminocyclohexanone and 11 g. of 2,4-dimethylphenylhydrazine hydrochloride there was obtained, after treatment of the free base in ether with ethereal hydrogen chloride, 10.9 g. of 3-(dimethylamino)-6,8-dimethyl-1,2,3,4-tetrahydrocarbazole hydrochloride; m.p. 312°-315° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04257952 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-5e4b5c1b59954dafbb9a0281d7e3910a |
| Source note | uspto-grants-1981_03 |