HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1281052Generated: October 31, 2026
Potassium Carbonate → 4-(6-Hydroxy-2,2,3,3,4,4,5,5-octafluorohexyloxy)benzaldehyde
https://huagongshe.com/reaction/1281052
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Fluorobenzaldehyde | HCID 68023 | — |
| Reactant | 2,2,3,3,4,4,5,5-Octafluorohexane-1,6-diol | HCID 136181 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | 4-(6-Hydroxy-2,2,3,3,4,4,5,5-octafluorohexyloxy)benzaldehyde | HCID 18546616 | — |
Reaction Steps
A mixture of 2,2,3,3,4,4,5,5-octafluoro-1,6-hexanediol (7.86 g), 4-fluorobenzaldehyde (1.24 g), NMP (10 mL), and potassium carbonate (4.14 g) was heated to 95-100° C. for 48 hrs. The mixture was further processed as described in Example 1 to provide 4-(6-hydroxy-2,2,3,3,4,4,5,5-octafluorohexyloxy)benzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06451960B1 |
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| Source dataset | uspto-grants-2002_09 |
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| ORD ID | ord-f5a35bd318e54be49d4a74748f3aa7cd |
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| Source note | uspto-grants-2002_09 |
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