HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 12874074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-(Dimethylamino)cyclohexan-1-one--hydrogen chloride (1/1) | HCID 12717448 | — |
| Reactant | (3-(Benzyloxy)phenyl)hydrazine hydrochloride | HCID 12891839 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 12874074 | HCID 12874074 | — |
Reaction Steps
A solution of 15.8 g. of 4-dimethylaminocyclohexanone hydrochloride and 20.3 g. of 3-benzyloxyphenylhydrazine hydrochloride (m.p. 165°-168° C.) in 225 ml. of absolute ethyl alcohol was heated under reflux for three hours, cooled to room temperature, and diluted with 50 ml. of water. After standing for three hours the resulting crystals were collected by filtration and washed with ethyl alcohol to give, after recrystallization from ethyl alcohol, 6.1 g. of 3-(dimethylamino)-7-(benzyloxy)-1,2,3,4-tetrahydrocarbazole hydrochloride, m.p. 237°-239° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04257952 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-f540a197607b4883af2442ebcef03c61 |
| Source note | uspto-grants-1981_03 |