Acrylic Acid → HCID 12084158, compound

HRID 1281200Notes

Reaction equation

[C:1]([OH:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]([NH:10][CH2:11][CH2:12][CH2:13][CH3:14])[CH2:7][CH2:8][CH3:9]>>[CH2:6]([N:10]([CH2:11][CH2:12][CH2:13][CH3:14])[CH2:3][CH2:2][C:1]([OH:5])=[O:4])[CH2:7][CH2:8][CH3:9]

Participants

Reactant 2

HCID 6581Acrylic Acid

HCID 8148Dibutylamine

Product 1

HCID 12084158HCID 12084158, compoundYield 98%

Procedure

After completion of the reaction, acrylic acid and di-n-butylamine were assayed by gas chromatography. As a result, formation of 152.5 g (yield 98%) of N,N-di-n-butyl-β-alanine was confirmed, with the rates of conversion of acrylic acid and di-n-butylamine being 98% and 98%, respectively.

Sources & evidence

ORD record: ord-eaf2b7ec09ab446dba10003f2a5daf38
Source dataset: uspto-grants-2002_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06452030B1

Reaction notes

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