HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86746863, compound → HCID 59910751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86746863 | HCID 86746863 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 59910751 | HCID 59910751 | 83.5% |
Reaction Steps
The compound (16-b)(0.272 g) was dissolved in acetic acid (10 ml). Zinc (3.5 g) was added little by little at room temperature, and the mixture was agitated for 2.5 hours. The crude product obtained by the conventional treatment of the reaction mixture was purified on silica gel column to give the titled compound (17-a) [yield:0.177 g(81%)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06452039B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-69d062cc3ccf4549894ec4b77e39ba78 |
| Source note | uspto-grants-2002_09 |