Sodium Hydroxide → HCID 9964564, compound

Participants

Reaction Steps

To a solution of diethyl 5-[(hydroxyamino)carbonyl]-1,3-benzenedicarboxylate (0.281 g, 1.0 mmol) in acetone (5 mL) was added 1.0 N NaOH (5 mL) at room temperature, and the mixture was stirred at room temperature for 2 hours. The solvent was removed under reduced pressure and the residue was taken up with 1 N HCl (15 nL) to give white precipitate. This material was dried under vacuum to give 0.096 g of white solid (43% yield).

Provenance & Evidence