HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69987001, compound → HCID 10143486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69987001 | HCID 69987001 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10143486 | HCID 10143486 | 66.7% |
Reaction Steps
4-[4-(2-{[(2S)-3-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxy-propyl]amino}ethyl)anilino]-N-(3-fluorobenzyl)-1-piperidinecarboxamide (0.174 g, 0.225 mmol) was reacted according to Procedure H (eluant: 5:1 chloroform-methanol containing 1% ammonium hydroxide) to give the title compound (0.085 g, 0.15 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451814B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-2873da4c82a34529a75eb8831e359654 |
| Source note | uspto-grants-2002_09 |