HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69985947, compound → HCID 10302915, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69985947 | HCID 69985947 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10302915 | HCID 10302915 | 62.5% |
Reaction Steps
4-[4-(2-{[(2S)-3-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxypropyl]amino}ethyl)anilino]-N-(2,6-difluorobenzyl)-1-piperidinecarboxamide (0.192 g, 0.24 mmol) was reacted according to Procedure H (eluant: 5:1 chloroform-methanol containing 1% ammonium hydroxide) to give the title compound (0.085 g, 0.15 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451814B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-4cc30071ef5f480c8a1b583251c504f6 |
| Source note | uspto-grants-2002_09 |