HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69985555, compound → HCID 69987371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69985555 | HCID 69985555 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 69987371 | HCID 69987371 | 71.4% |
Reaction Steps
1-{4-[4-(2-{[(2S)-3-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxypropyl]-amino}ethyl)anilino]-1-piperidinyl}-1-hexanone (0.13 g, 0.168 mmol) was reacted according to Procedure H (eluant: 5:1 chloroform-methanol containing 1% ammonium hydroxide) to give the title compound (0.058 g, 0.120 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451814B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-48c0294486b04194938f17564993ed6a |
| Source note | uspto-grants-2002_09 |