HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluoronitrobenzene → HCID 18422367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluoronitrobenzene | HCID 67967 | — |
| Reactant | HCID 18422199 | HCID 18422199 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 18422367 | HCID 18422367 | — |
Reaction Steps
In the same manner as in Starting Material Synthesis Example 4 and using methyl 2-amino-5-methylbenzo[b]thiophene-3-carboxylate (3.11 g), 2,4-difluoronitrobenzene (1.54 ml) and dimethyl sulfoxide (30 ml), methyl 2-(5-fluoro-2-nitroanilino)-5-methylbenzo[b]thiophene-3-carboxylate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455521B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-456797e46c7b46efb01e321ce88a14e3 |
| Source note | uspto-grants-2002_09 |