HCID 86737625, compound → HCID 23431698, compound

HRID 128178Notes

Reaction equation

HRID 128178 reaction equation
[N+:1]([C:4]1[CH:14]=[C:13]([N+:15]([O-])=O)[CH:12]=[CH:11][C:5]=1[O:6][CH:7]([OH:10])[CH2:8][CH3:9])([O-])=O.[H][H]>>[NH2:1][C:4]1[CH:14]=[C:13]([NH2:15])[CH:12]=[CH:11][C:5]=1[O:6][CH:7]([OH:10])[CH2:8][CH3:9]

Participants

3

Reactant 2

HCID 86737625HCID 86737625, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 23431698HCID 23431698, compound

Procedure

0.039 mol (9.5 g) of (2,4-dinitro) phenoxypropanol in 30 cm3 of absolute alcohol are reduced on Pd/C at 10% in a bomb under 25 kg of pressure of hydrogen at 70° C. for 1 hour.

Sources & evidence

ORD record
ord-6637bed5c0d54a108f20328edf9d95eb
Source dataset
uspto-grants-1981_03
Patent number
US04259261

Reaction notes

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