1-Fluoro-2-nitrobenzene → HCID 18422357, compound

HRID 1281810Notes

Reaction equation

HRID 1281810 reaction equation
[NH2:1][C:2]1[S:6][C:5]2[CH:7]=[C:8]([Cl:11])[CH:9]=[CH:10][C:4]=2[C:3]=1[C:12]#[N:13].F[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[N+:21]([O-:23])=[O:22]>>[Cl:11][C:8]1[CH:9]=[CH:10][C:4]2[C:3]([C:12]#[N:13])=[C:2]([NH:1][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[N+:21]([O-:23])=[O:22])[S:6][C:5]=2[CH:7]=1

Participants

3

Reactant 2

HCID 738951-Fluoro-2-nitrobenzeneHCID 184223152-Amino-6-chloro-1-benzothiophene-3-carbonitrile

Product 1

HCID 18422357HCID 18422357, compound

Procedure

In the same manner as in Starting Material Synthesis Example 51 and using 2-amino-6-chlorobenzo[b]thiophene-3-carbonitrile and 2-fluoronitrobenzene, 6-chloro-2-(2-nitroanilino)benzo[b]thiophene-3-carbonitrile is obtained.

Workup

  1. customMaterial Synthesis Example 51

Sources & evidence

ORD record
ord-7dc0eaf4c09844e787e8fe240ee705b5
Source dataset
uspto-grants-2002_09
Patent number
US06455521B1

Reaction notes

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