HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Ethanedithiol → HCID 18422249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Ethanedithiol | HCID 33645 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 18422372 | HCID 18422372 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18422249 | HCID 18422249 | — |
Reaction Steps
In the same manner as in Example 62 and using 8-fluoro-1-methoxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine, dichloromethane, ethanedithiol and aluminium chloride, 8-fluoro-1-hydroxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455521B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-f9161c57c1f34e36afcf94a8418d40c0 |
| Source note | uspto-grants-2002_09 |