HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Ethanedithiol → HCID 18422353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Ethanedithiol | HCID 33645 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 18422226 | HCID 18422226 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18422353 | HCID 18422353 | — |
Reaction Steps
In the same manner as in Example 62 and using 8-fluoro-2-methoxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine, dichloromethane, ethanedithiol and aluminium chloride, 8-fluoro-2-hydroxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455521B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-6d37b1e46aca45bcbe1310693354d20c |
| Source note | uspto-grants-2002_09 |